分散液液微萃取-高效液相色谱法联用检测豆浆中双酚A的质量浓度

doi:10.3969/j.issn.1007-2861.2015.03.010

Abstract

Abstract:

A novel method was developed for determination of bisphenol A in soybean milk using dispersive liquid-liquid microextraction coupled with high performance liquid chromatography (DLLME-HPLC). Under the optimal conditions, the peak area had a linear relation with the concentration of bisphenol A over the range of 1~100 μg/L. The detection limit was 0.3 μg/L and recovery was among 91.6%~97.5%. The method had good accuracy and reproducibility, and was appropriate for determination of bisphenol A in soybean milk.

Key words: dispersive liquid-liquid microextraction (DLLME) , high performance liquid chromatography (HPLC) , soybean milk, bisphenol A

ZHA Yiming, WANG Xinxiu, FAN Yong, WANG Tianlin, LUO Liqiang. Determination of bisphenol A in soybean milk by dispersive liquid-liquid microextraction coupled with high performance liquid chromatography[J]. Journal of Shanghai University（Natural Science Edition）, 2016, 22(6): 746-752.

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Determination of bisphenol A in soybean milk by dispersive liquid-liquid microextraction coupled with high performance liquid chromatography

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