上海大学学报(自然科学版) ›› 2012, Vol. 18 ›› Issue (3): 327-330.doi: 10.3969/j.issn.1007-2861.2012.03.021

• 论文 • 上一篇    

多循环快速热退火诱导普通玻璃衬底非晶硅薄膜晶化

於凡枫,金晶,史伟民,瞿晓雷,许月阳   

  1. (上海大学 材料科学与工程学院,上海 200072)
  • 出版日期:2012-06-30 发布日期:2012-06-30
  • 通讯作者: 金晶(1979~),女,博士,研究方向为半导体材料及其光电器件. E-mail:jjin@shu.edu.cn
  • 基金资助:

    上海市重点学科建设资助项目(S30107)

Crystallization of Amorphous Silicon Films on Glass Substrate by Multi-cycle Rapid Thermal Annealing

YU Fan-feng,JIN Jing,SHI Wei-min,QU Xiao-lei,XU Yue-yang   

  1. (School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China)
  • Online:2012-06-30 Published:2012-06-30

摘要: 介绍一种使用快速热退火设备,经多次循环退火诱导,在普通玻璃衬底上生长非晶硅薄膜晶化的实验方法.利用拉曼(Raman)光谱、原子力显微镜(atomic force microscope,AFM)、紫外可见分光光度计(UV-VIS spectrophotometer)和霍尔(Hall)测试系统对薄膜的结构、形貌及电子迁移率进行测试.结果表明,当退火温度达到680 ℃时,薄膜开始出现晶化现象;随着快速热退火次数的增加,拉曼光谱在500 cm-1处测得多晶硅特征峰;在循环退火5次后,其最佳晶化率达到71.9%,光学带隙下降,晶粒增大,载流子迁移率提高.

关键词: 多循环快速热退火, 非晶硅, 晶化

Abstract: This paper introduces a method of multicycle rapid thermal annealing that induces crystallization of amorphous silicon films deposited on the normal glass. The structure, surface morphology and electron mobility of the silicon films were investigated with Raman spectra, atomic force microscope (AFM), UV-VIS spectrophotometer and Halleffect measurements. The results show that the crystallization appears for films annealed at 680 ℃. As rapid thermal annealing cycles are increased, the Raman spectra indicate that the characteristic peak of polycrystalline silicon (poly-Si) film appears at 500 cm-1. The maximal crystalline fraction of polySi film is 71.9% after 5 cycles annealing treatment. The optical band gap decreases with the grain growing, and the carrier mobility increases.

Key words: amorphous silicon, crystallization, multi-cycle rapid thermal annealing

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