上海大学学报(自然科学版) ›› 2011, Vol. 17 ›› Issue (4): 514-521.doi: 10.3969/j.issn.1007-2861.2011.04.018

• 材料科学 • 上一篇    下一篇

微纳液滴的凝固及熔化特性研究

高玉来,翟启杰,徐匡迪   

  1. (上海大学 材料科学与工程学院,上海 200072)
  • 出版日期:2011-08-30 发布日期:2011-08-30
  • 通讯作者: 高玉来(1975~),男,教授,博士生导师,博士,研究方向为微纳液滴凝固和熔化特性、纳米材料的制备与表征. E-mail:ylgao@shu.edu.cn
  • 基金资助:

    国家自然科学基金资助项目(50401023,50571057,50971086; 上海市纳米专项基金资助项目(0452NM062);上海市青年科技启明星计划资助项目(06QA14020; 上海市AM基金资助项目(08520740500);Robert Bosch Foundation(32.5.8003.0025.0/MA01)

Research on Solidification and Melting Characteristics of Micro and Nano sized Droplets

GAO Yu-lai,ZHAI Qi-jie,XU Kuang-di   

  1. (School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China)
  • Online:2011-08-30 Published:2011-08-30

摘要: 金属的凝固和熔化是金属材料成形过程中的重要相变过程.当大体积的金属熔体被弥散为尺度在微米乃至纳米的微小液滴时,金属的凝固和熔化均会由于材料自身尺度的减小,而在相变过程中发生显著的变化.这一过程涉及到基础科学问题的研究、样品制备及表征技术的开发等,对金属的最终组织和使用性能,也会产生显著影响.对本研究团队近年来在微纳液滴凝固及熔化特性方面的研究进行总结,同时对该研究领域未来的发展进行展望.

关键词: 尺寸效应, 金属凝固, 纳米量热仪, 微纳液滴, 无铅焊料

Abstract: Solidification and melting of metallic materials are crucial phase transformation in the metal forming process. When metallic materials in bulk volume are dispersed into infinitesimal droplets in microsize or even nanosize, significant changes in the solidification and melting processes can occur due to the size reduction of the materials. Obviously, these changes will dramatically influence the structure and service performances of the metallic materials. In this process, fundamental research on the scientific issues and the preparation techniques and characteristic methods for metallic droplets are involved. This article summarizes the research activities and accomplishments of the group in solidification and melting characteristics of infinitesimal droplets. Besides, the future development of research in this field is prospected.

Key words: metal solidification, micro and nano sized droplet, nanocalorimetry, Pbfree solder, size effect

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