Journal of Shanghai University(Natural Science Edition) ›› 2010, Vol. 16 ›› Issue (1): 97-104.
• Civil Engineering • Previous Articles Next Articles
HU Long-xing,CHEN Yong-feng,XU Jia-jia
Received:
Online:
Published:
Abstract:
The mesoporous molecular sieves MCM-41 and SBA-15 with spherical morphology were synthesized. The samples were characterized by XRD, N2 adsorptiondesorption analysis, SEM and TEM. The results show that the samples prepared in the research have the same typical parameters as those of the conventional hydrothermal method. The prepared MCM-41 and SBA-15 have the specific surface areas of 1 107 m2·g-1and 583 m2·g-1, respectively, the specific pore volumes of 0.69 cm3·g-1and 1.27 cm3·g-1 respectively, and the average pore diameters of 2.5 nm and 7.4 nm respectively. Both MCM-41 and SBA-15 prepared have good spherical morphology. The wet grinding process had little effect on the morphology of MCM-41, but great effect on the spherical morphology of SBA-15. The ordered internal pore channel structure could be observed only after wet grinding because of the larger particle size of SBA-15.
Key words: MCM-41; SBA-15; synthesis and characterization; morphology control
CLC Number:
TB 383
HU Long-xing,CHEN Yong-feng,XU Jia-jia. Synthesis and Characterization of Mesoporous Silica with Spherical Morphology[J]. Journal of Shanghai University(Natural Science Edition), 2010, 16(1): 97-104.
0 / / Recommend
Add to citation manager EndNote|Reference Manager|ProCite|BibTeX|RefWorks
URL: https://www.journal.shu.edu.cn/EN/
https://www.journal.shu.edu.cn/EN/Y2010/V16/I1/97