顶空固相微萃取联合气相色谱法测定土壤中30种卤代烃化合物的方法

doi:10.3969/j.issn.1007-2861.2015.03.012

Abstract

Abstract:

This paper studies an analytical technique of 30 halogenated hydrocarbon compounds in soil using a method of head space solid phase micro-extraction (HS-SPME), and analyzes influencing factors of target extraction efficiency. As a result, optimum extraction conditions are determined within 0.25~50.0×10³ ng/L, with good linearity. The detection limit is 0.04~3.58×10³ ng/kg. Blank standard addition recovery is 62.7%~122.0%, and relative standard deviation (RSD) is 0.7%~14.9%.

Key words: halogenated hydrocarbon compound , gas chromatograph, head space solid phase microextraction(HS-SPME) , soil

PEI Yongqiang, FAN Zhanchun, ZHAO Jing, YUE Jianwei, LI Yongqing, LI Huanfeng. Determination of 30 halogenated hydrocarbon compounds in soil with head space solid phase micro-extraction and gas chromatography[J]. Journal of Shanghai University（Natural Science Edition）, 2017, 23(1): 112-120.

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Determination of 30 halogenated hydrocarbon compounds in soil with head space solid phase micro-extraction and gas chromatography

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